Validation for simultaneous determination of tetracycline by using QuEChERS method and LC-MS/MS in liver of buffalo
Date
10/06/2017
Journal Title
Journal ISSN
Volume Title
Type
Article
Publisher
New York Science Journal
Series Info
New York Science Journal;
Scientific Journal Rankings
Abstract
The aim of this study is to determine a method validation for the presence of tetracycline antibiotics (Tetracycline (TC), Oxytetracycline (OTC), Chlortetracycline (CTC) and Doxycycline (DOC) in liver tissue of buffalo. LC-MS/MS was used for determination of tetracycline antibiotic residues. Separation was carried out by with electrospray ionization (ESI) in positive -ion mode using mobile phase at a flow rate of 400 ml/min and injection volume 5 ul. The recoveries of analyzed drugs were in between 75 and 80 ppb
[Kamal Magdy Kamal, Amgad Mostafa Rady, Lamia Ryad, and Nermine Gad Validation for simultaneous determination of tetracycline by using QuEChERS method and LC-MS/MS in liver of buffalo N Y Sci
Description
MSA Google Scholar
Keywords
Tetracyclines, LC-MS/MS, validation, EU commission
Citation
1- Alfredsson, G., Branzell, C., Granelli, K., & Lundström, Å. (2005). Simple and rapid screening and confirmation of tetracyclines in honey and egg by a dipstick test and LC–MS/MS. Analytica Chimica Acta, 529(1), 47-51. 2- Andersen, W. C., Roybal, J. E., Gonzales, S. A., Turnipseed, S. B., Pfenning, A. P., & Kuck, L. R. (2005). Determination of tetracycline residues in shrimp and whole milk using liquid chromatography with ultraviolet detection and residue confirmation by mass spectrometry. Analytica Chimica Acta, 529(1), 145-150. 3- Andreu, V., Vazquez-Roig, P., Blasco, C., & Picó, Y. (2009). Determination of tetracycline residues in soil by pressurized liquid extraction and liquid chromatography tandem mass spectrometry. Analytical and bioanalytical chemistry, 394(5), 1329-1339. 4- Blasco, C., Di Corcia, A., & Picó, Y. (2009). Determination of tetracyclines in multi-specie animal tissues by pressurized liquid extraction and liquid chromatography–tandem mass spectrometry. Food Chemistry, 116(4), 1005-1012. 5- Cháfer-Pericás, C., Maquieira, Á., Puchades, R., Miralles, J., & Moreno, A. (2013). Multiresidue determination of antibiotics in feed and fish samples for food safety evaluation. Comparison of immunoassay vs LC-MS-MS. Food Control, 22(6), 993-999. 6- EUROPEAN COMMISSION REGULATION (2010) NO 37/2010 of 26 January 2010 on aying down requirements on the quality of aeronautical data and aeronautical information for the single European sky, Official Journal of the European Unionl15/19 P.9-10 7- Lopez, M. I., Pettis, J. S., Smith, I. B., & Chu, P. S. (2014). Multiclass determination and confirmation of antibiotic residues in honey using LC-MS/MS. Journal of agricultural and food chemistry, 56(5), 1553-1559. 8- Nakazawa, H., Ino, S., Kato, K., Watanabe, T., Ito, Y., & Oka, H. (1999). Simultaneous determination of residual tetracyclines in foods by high-performance liquid chromatography with atmospheric pressure chemical ionization tandem mass spectrometry. Journal of Chromatography B: Biomedical Sciences and Applications, 732(1), 55-64. 9- Samanidou, V. F., Nikolaidou, K. I., & Papadoyannis, I. N. (2009). Development and validation of an HPLC confirmatory method for the determination of seven tetracycline antibiotics residues in milk according to the European Union Decision 2002/657/EC. Journal of separation science,30(15), 2430-2439. 10- Yang, S., Cha, J., & Carlson, K. (2004). Quantitative determination of trace concentrations of tetracycline and sulfonamide antibiotics in surface water using solid‐phase extraction and liquid chromatography/ion trap tandem mass spectrometry. Rapid communications in mass spectrometry, 18(18), 2131-2145. 11- Zhu, J., Snow, D. D., Cassada, D. A., Monson, S. J., & Spalding, R. F. (2009). Analysis of oxytetracycline, tetracycline, and chlortetracycline in water using solid-phase extraction and liquid chromatography–tandem mass spectrometry. Journal of Chromatography A, 928(2), 177-186.