Simultaneous Determination of Five Coccidiostats in Veterinary Powders, Feed Premixes, and Baby Food by Micellar Electrokinetic Chromatography: Application to Chicken Tissues and Liver

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dc.AffiliationOctober University for modern sciences and Arts (MSA)
dc.contributor.authorBelal F.
dc.contributor.authorEl-Razeq S.A.
dc.contributor.authorFouad M.
dc.contributor.authorZayed S.
dc.contributor.authorFouad F.
dc.contributor.otherDepartment of Pharmaceutical Analytical Chemistry
dc.contributor.otherFaculty of Pharmacy
dc.contributor.otherUniversity of Mansoura
dc.contributor.otherMansoura
dc.contributor.otherEgypt; Department of Analytical Chemistry
dc.contributor.otherFaculty of Pharmacy
dc.contributor.otherAl-Azhar University
dc.contributor.otherCairo
dc.contributor.otherEgypt; Department of Analytical Chemistry
dc.contributor.otherFaculty of Pharmacy
dc.contributor.otherAl-Azhar University
dc.contributor.otherOctober University for Modern Sciences and Arts
dc.contributor.otherCairo
dc.contributor.otherEgypt; Unit of Drug Analysis
dc.contributor.otherFaculty of Pharmacy
dc.contributor.otherUniversity of Mansoura
dc.contributor.otherMansoura
dc.contributor.otherEgypt
dc.date.accessioned2020-01-09T20:40:48Z
dc.date.available2020-01-09T20:40:48Z
dc.date.issued2018
dc.descriptionScopus
dc.description.abstractA new, simple, and reliable micellar electrokinetic chromatographic method was developed and validated for the simultaneous determination of amprolium, ethopabate, diaveridine, sulphadimidine, and sulphaquinoxaline. The separation was achieved using 50�mM tris buffer (pH 8.5) with 50�mM SDS and 15% acetonitrile (v/v) at 28�kV and the components were detected at 200�nm. Different factors affecting the electrophoretic mobility of the five investigated drugs were studied and optimized. Method validation showed that calibration plots were linear within the range from 0.5 to 100�?g/mL with a correlation coefficient > 0.998. Intraday and interday precision and accuracy evaluated by relative standard deviation were lower than 2%. The limits of detection were in the ranges of 0.02 to 0.07�?g/mL. The new method with simple sample pretreatment based on aqueous methanol extraction has been successfully applied for analysis of these drugs in powder preparations, feed premixes, baby food, chicken tissues, and liver samples with the recoveries of 97�101%. The present method is suitable and favorable for the analysis of the five coccidiostats drugs on account of its cost effectiveness, simplicity, rapidity, and sensitivity. � 2018, Springer Science+Business Media, LLC, part of Springer Nature.en_US
dc.description.urihttps://www.scimagojr.com/journalsearch.php?q=14500154701&tip=sid&clean=0
dc.identifier.doihttps://doi.org/10.1007/s12161-018-1330-y
dc.identifier.doiPubMed ID :
dc.identifier.issn19369751
dc.identifier.otherhttps://doi.org/10.1007/s12161-018-1330-y
dc.identifier.otherPubMed ID :
dc.identifier.urihttps://t.ly/kNxZA
dc.language.isoEnglishen_US
dc.publisherSpringer New York LLCen_US
dc.relation.ispartofseriesFood Analytical Methods
dc.relation.ispartofseries11
dc.subjectOctober University for Modern Sciences and Arts
dc.subjectUniversity for Modern Sciences and Arts
dc.subjectMSA University
dc.subjectجامعة أكتوبر للعلوم الحديثة والآداب
dc.subjectAnticoccidial drugsen_US
dc.subjectBaby fooden_US
dc.subjectChicken tissuesen_US
dc.subjectFeed premixesen_US
dc.subjectLiveren_US
dc.subjectMicellar electrokinetic chromatographyen_US
dc.subjectPowder preparationsen_US
dc.subjectAnimalsen_US
dc.subjectChromatographic analysisen_US
dc.subjectCost effectivenessen_US
dc.subjectElectrodynamicsen_US
dc.subjectElectrophoretic mobilityen_US
dc.subjectHistologyen_US
dc.subjectLiquid chromatographyen_US
dc.subjectLiveren_US
dc.subjectTissueen_US
dc.subjectAnticoccidial drugsen_US
dc.subjectBaby foodsen_US
dc.subjectChicken tissueen_US
dc.subjectMicellar electrokinetic chromatographyen_US
dc.subjectPowder preparationen_US
dc.subjectMeatsen_US
dc.titleSimultaneous Determination of Five Coccidiostats in Veterinary Powders, Feed Premixes, and Baby Food by Micellar Electrokinetic Chromatography: Application to Chicken Tissues and Liveren_US
dc.typeArticleen_US
dcterms.isReferencedByAbd-El-Sattar, O.A., Simultaneous determination of sulphaquinoxaline and amprolium in veterinary mixture by HPLC and first derivative ultraviolet spectrophotometry (2002) Saudi Pharm J, 10 (4), pp. 190-195; Aguilera-Luiz, M.M., Martenez Vidal, J.I., Romero-Gonzllez, R., Garrido Frenich, A., Multiclass method for fast determination of veterinary drug residues in baby food by ultra-high-performance liquid chromatography�tandem mass spectrometry (2012) Food Chem, 132, pp. 2171-2180. , COI: 1:CAS:528:DC%2BC38Xit1Wnur8%3D; Alomary, A., Simultaneous quantification of amprolium and ethopabate in pharmaceutical preparation by derivative ultraviolt spectroscopy (2004) Abhath Al-Yarmouk Pure Science and Engineering Series, 13 (1), pp. 59-70. , COI: 1:CAS:528:DC%2BD2cXms1OksLw%3D; Belal, F., Sharaf El-Din, M.K., Tolba, M., El-Awady, M., El-Mansi, H., Analysis of four antimigraine drugs in two ternary mixtures by sweeping-micellar electrokinetic chromatography with retention factor gradient effect and dynamic pH junction (2016) Microchem J, 127, pp. 11-21. , COI: 1:CAS:528:DC%2BC28Xhsl2rtLY%3D; Broekaert, N., Van Peteghem, C., Daeseleire, E., Sticker, D., Van Poucke, C., Development and validation of an UPLC-MS/MS method for the determination of ionophoric and synthetic coccidiostats in vegetables (2011) Anal Bioanal Chem, 401, pp. 3335-3344. , COI: 1:CAS:528:DC%2BC3MXht1ygs7nK; Ching-Erh, L., Migration behavior and separation of sulfonamides in capillary zone electrophoresis III. Citrate buffer as a background electrolyte (1997) J Chromatogr A, 768 (1), pp. 105-112; Clarke, L., Fodey, T.L., Crooks, S.R.H., Moloney, M., O'Mahony, J., Delahaut, P., O�Kennedy, R., Danaher, M., A review of coccidiostats and the analysis of their residues in meat and other food (2014) Meat Sci, 97, pp. 358-374. , COI: 1:CAS:528:DC%2BC2cXislKqtLc%3D; (2005), Commission Recommendation 2005/925/EC, Off J Eur Commun L337/51; El-Awady, M., Belal, F., Pyell, U., Robust method for the analysis of hydrophobic base analytes loratadine and desloratadinein pharmaceutical preparations and biological fluids by sweeping-cyclodextrin modified micellar electrokinetic chromatography (2013) J Chromatogr A, 1309, pp. 64-75. , COI: 1:CAS:528:DC%2BC3sXht1yhsL%2FF; El-Kosasy, A.M., Hussein, L.A., Magdy, N., Abbas, M.M., Sensitive spectrofluorimetric methods for determination of ethopabate and amprolium hydrochloride in chicken plasma and their residues in food samples (2015) Spectrochim Acta A Mol Biomol Spectrosc, 150, pp. 430-439. , COI: 1:CAS:528:DC%2BC2MXpt12iu70%3D; Commission Regulation No 37/2010 of 22nd December 2009 on pharmacologically active substances and their classification regarding maximum residue limits in foodstuffs of animal origin (2010) Off J Eur Communities, L15, p. 1, 72; Font, G., Juan-Garc�a, A., Pic�, Y., Pressurized liquid extraction combined with capillary electrophoresis�mass spectrometry as an improved methodology for the determination of sulfonamide residues in meat (2007) J Chromatogr A, 1159 (1-2), pp. 233-241. , COI: 1:CAS:528:DC%2BD2sXnslGgtb0%3D; Furusawa, N., Simplified high-performance liquid chromatographic determination of residual amprolium in edible chicken tissues (2002) J Chromatogr Sci, 40, pp. 355-358; Ghanem, M., Abu-Lafi, S., Validation of a stability-indicating assay of amprolium hydrochloride in water soluble powder formulation using hydrophilic interaction liquid chromatography (2013) J Appl Pharm Sci, 3 (10), pp. 51-58. , COI: 1:CAS:528:DC%2BC2cXmvVClt7k%3D; Girardi, C., Odore, R., Pharmacological treatments and risks for the food chain (2008) Vet Res Commun, 32, p. S11; Hartig, C., Storm, T., Jekel, M., Detection and identification of sulphonamide drugs in municipal waste water by liquid chromatography coupled with electrospray ionisation tandem mass spectrometry (1999) J Chromatogr A, 854, pp. 163-173. , COI: 1:CAS:528:DyaK1MXmsVSisr8%3D; Heiger, D.N., (1992) An introduction high performance capillary electrophoresis, , 2, Hewlett-Packard Company, France; Hows, M.E.P., Perrett, D., Kay, J., Optimization of a simultaneous separation of sulphonamides, dihydrofolate reductase inhibitors and ?-lactam antibiotics by capillary electrophoresis (1997) J Chromatogr A, 768, pp. 97-104. , COI: 1:CAS:528:DyaK2sXisVelsrg%3D; Hussein, L.A., Magdy, N., Abbas, M.M., Five different spectrophotometric methods for determination of amprolium hydrochloride and ethopabate binary mixture (2015) Spectrochim Acta A Mol Biomol Spectrosc, 138, pp. 395-405. , COI: 1:CAS:528:DC%2BC2cXitVKqt77N; (2005) Technical requirements for the registration of pharmaceutical for human use, validation of analytical procedures; text and methodology Q2 (R1), pp. 1-13. , Geneva; Kaklamanos, G., Vincent, U., Von Holst, C., Analysis of antimicrobial agents in pig feed by liquid chromatography coupled to orbitrap mass spectrometry (2013) J Chromatogr A, 1293, pp. 60-74; Kao, Y., Chang, M., Cheng, C., Chou, S., Multiresidue determination of veterinary drugs in chicken and swine muscles by high performance liquid chromatography (2001) J Food Drug Anal, 9 (2), pp. 84-95. , COI: 1:CAS:528:DC%2BD3MXmvFSktb4%3D; Kim, B., Ham, H., Lee, J., Cheong, N., Myung, S., Determination of coccidiostats (amprolium and decoquinate) in cattle and chicken�s muscle using high performance liquid chromatography (2012) Bull Kor Chem Soc, 33 (2), pp. 559-563. , COI: 1:CAS:528:DC%2BC38XktFOmtLs%3D; K?iv�nkov�, L., Bo?ek, P., Determination of amprolium in feed stuff by capiliary isotachophoresis (1985) Electrophoresis, 6 (3), pp. 143-144; Liu, R., He, P., Li, Z., Li, R., Simultaneous determination of 16 sulfonamides in animal feeds by UHPLC�MS�MS (2011) J Chromatogr Sci, 49 (8), pp. 640-646. , COI: 1:CAS:528:DC%2BC3MXhtVKisbnI; Martinez-Villalba, A., Moyano, E., Teresa Galceran, M., Analysis of amprolium by hydrophilic interaction liquid chromatography�tandem mass spectrometry (2010) J Chromatogr A, 1217, pp. 5802-5807. , COI: 1:CAS:528:DC%2BC3cXhtVKgsbfK; Mart�nez-Villalba, A., Nunez, O., Moyano, E., Teresa Galceran, M., Field amplified sample injection-capillary zone electrophoresis for the analysis of amprolium in eggs (2013) Electrophoresis, 34, pp. 870-876; Mcevoy, J.D.G., Contamination of animal feedingstuffs as a cause of residues in food: a review of regulatory aspects, incidence and control (2002) Anal Chim Acta, 473, pp. 3-26, 2002. , COI: 1:CAS:528:DC%2BD38XosVKgs7s%3D; Nasr, J.J., Shalan, S., Spectrofluorimetric analysis of ethopabate in veterinary formulations with application to residue determination in chicken muscles and liver (2014) Luminescence, 29 (8), pp. 1188-1193. , COI: 1:CAS:528:DC%2BC2cXitFSqtLnN; Nour El-Dien, F.A., Mohamed, G.G., Khaled, E., Frag, E.Y.Z., Extractive spectrophotometric determination of sulphonamide drugs in pure and pharmaceutical preparations through ion-pair formation with molybdenum(V) thiocyanate in acidic medium (2010) J Adv Res, 1, pp. 215-220; Ortelli, D., Cognard, E., Jan, P., Edder, P., Comprehensive fast multiresidue screening of 150 veterinary drugs in milk by ultra-performance liquid chromatography coupled to time of flight mass spectrometry (2009) J Chromatogr B, 877, pp. 2363-2374. , COI: 1:CAS:528:DC%2BD1MXoslehu7s%3D; Petersa, R.J.B., Bolcka, Y.J.C., Rutgersa, P., Stolkera, A.A.M., Nielena, M.W.F., Multi-residue screening of veterinary drugs in egg, fish and meat using high-resolution liquid chromatography accurate mass time-of-flight mass spectrometry (2009) J Chromatogr A, 1216, pp. 8206-8216; Riekkola, M.L., Joensson, J.A., Smith, R.M., Terminology for analytical capillary electromigration techniques (IUPAC Recommendations 2003) (2004) Pure Appl Chem, 76 (2), pp. 443-451. , COI: 1:CAS:528:DC%2BD2cXjtVeitb4%3D; Rizk, M.S., Zaky Frag, E.Y., Mohamed, G.G., Tamam, A.A., Spectrophotometric determination of distigmine bromide, cyclopentolate HCL, diaveridine HCL and tetrahydrozoline HCL via charge-transfer complex formation DDQ reagent (2013) Iran J Pharm Res, 3 (2), pp. 168-183. , COI: 1:CAS:528:DC%2BC3sXntVOjtL8%3D; Salama, N.N., Fouad, M.M., Rashed, N.M., Validated chromatographic methods for simultaneous determinations of amprolium hydrochloride and ethopabate in veterinary preparations (2012) IJPBR, 3 (4), pp. 185-190. , COI: 1:CAS:528:DC%2BC38Xhs1OitrbN; Smallidge, R.L., Jr., Gas-liquid chromatographic determination of ethopabate in feed premixes (1978) J Assoc Off Anal Chem, 61 (3), pp. 561-563. , COI: 1:CAS:528:DyaE1cXkslChtLc%3D, PID: 649547; Song, W., Huang, M., Rumbeiha, W., Li, H., Determination of amprolium, carbadox, monensin, and tylosin in surface water by liquid chromatography/tandem mass spectrometry (2007) Rapid Commun Mass Spectrom, 21, pp. 1944-1950. , COI: 1:CAS:528:DC%2BD2sXmvVamu74%3D; Springer, V.H., Lista, A.G., Micellar nanotubes dispersed electrokinetic chromatography for the simultaneous determination of antibiotics in bovine milk (2012) Electrophoresis, 33 (13), pp. 2049-2055. , COI: 1:CAS:528:DC%2BC38XhtVehtrnO; Van Rhijna, J.A., Lasaromsa, J.J.P., Berendsena, B.J.A., Brinkmanb, U.A.T., Liquid chromatographic�tandem mass spectrometric determination of selected sulphonamides in milk (2002) J Chromatogr A, 960, pp. 121-133; Vinay, K., Pardeep, S., Pawan, K., Mehlabs, S., Anu, G., Vijayta, G., Anticoccidial drugs used in the poultry: an overview (2013) Sci Int, 7, pp. 261-265; Wanga, H., Yuana, B., Zenga, Z., Hea, L., Dinga, H., Guoa, C., Konga, X., Huang, X., Identification and elucidation of the structure of in vivo metabolites of diaveridine in chicken (2014) J Chromatogr B, 965, pp. 91-99
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