Advanced Amplitude Centering as an invigorating Manipulation for Unifird Wavelength
Date
2017
Authors
Journal Title
Journal ISSN
Volume Title
Type
Article
Publisher
NNOVARE
Series Info
International Journal of Pharmacy and Pharmaceutical Sciences;Vol 9, Issue 5, 2017
Doi
Scientific Journal Rankings
Abstract
Objective: This work presented the novel spectrophotometric approach namely, advanced amplitude centering (AAC). The method was applied forthe resolution of ternary mixtures with partially or completely overlapped spectra.Methods: Advanced amplitude centering was based on the determination of ternary mixtures using single divisor where the concentrations of thecomponents are determined through progressive manipulation performed on the same ratio spectrum. The centered amplitude at unified wavelength was resolved and applied for the determination of three components with partially and severely overlapped spectra. The work discussed the applications and advantages of the novel univariate advanced amplitude centering compared to the chemometric model, partial least square (PLS).Results: The specificity of the proposed methods was checked using laboratory-prepared mixtures of amlodipine (AML), valsartan (VAL) and hydrochlorothiazide (HCT) and was successfully applied for the analysis of two pharmaceutical formulations. The validity of results was assessed by applying the standard addition technique. Conclusion: The results obtained were found to agree statistically with those obtained by a reported method, showing no significant difference with respect to accuracy and precision.
Description
Keywords
Resolution of mixtures, Hydrochlorothiazide, Valsartan, Amlodipine, Severely overlapping spectra, Amplitude centering
Citation
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