Qualitative and quantitative chemometry as stability-indicating methods for determination of dantrolene sodium and paracetamol

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dc.AffiliationOctober University for modern sciences and Arts (MSA)
dc.contributor.authorYehia A.M.
dc.contributor.authorSami I.
dc.contributor.authorRiad S.M.
dc.contributor.authorEl-Saharty Y.S.
dc.contributor.otherCairo University
dc.contributor.otherFaculty of Pharmacy
dc.contributor.otherDepartment of Analytical Chemistry
dc.contributor.otherKasr El-Aini Street
dc.contributor.otherCairo
dc.contributor.otherET 11562
dc.contributor.otherEgypt; October University for Modern Sciences and Arts
dc.contributor.otherFaculty of Pharmacy
dc.contributor.otherPharmaceutical Analytical Chemistry Department
dc.contributor.other6 October City
dc.contributor.other11787
dc.contributor.otherEgypt
dc.date.accessioned2020-01-09T20:41:07Z
dc.date.available2020-01-09T20:41:07Z
dc.date.issued2018
dc.descriptionScopus
dc.description.abstractBackground: Simultaneous determination of binary mixtures with simple and cost effective analysis is always of interest. Progressive advancement in chemometrics enables spectral resolution of drugs in the presence of their degradation products or impurities. Methods and Result: Three stability indicating chemometric methods are applied for the simultaneous determination of Dantrolene sodium (DNT) and Paracetamol (PAR). Partial Least Squares (PLS), Concentration Residuals Augmented Classical Least Squares (CRACLS) and Multivariate Curve Resolution-Alternating Least Squares (MCR-ALS) were selected for that purpose. DNT and PAR were determined in the linearity range of (2 � 10 ?g mL-1) and (12 � 28 ?g mL-1), respectively, in the presence of their degradation products. The presented methods were compared for their qualitative and quantitative analyses and validated according to the ICH guidelines. Furthermore, statistical comparison between the results obtained by the proposed methods and the reported chromatographic method showed no significant differences. Conclusion: The proposed multivariate calibrations were accurate and specific for quantitative analysis of the studied components. Furthermore, CRACLS and MCR-ALS methods succeeded in both quantitative and qualitative of the studied components and their degradation products. � 2018 Bentham Science Publishers.en_US
dc.description.urihttps://www.scimagojr.com/journalsearch.php?q=4700152426&tip=sid&clean=0
dc.identifier.doihttps://doi.org/10.2174/1573412913666170109155812
dc.identifier.doiPubMed ID :
dc.identifier.issn15734129
dc.identifier.otherhttps://doi.org/10.2174/1573412913666170109155812
dc.identifier.otherPubMed ID :
dc.identifier.urihttps://t.ly/veLLq
dc.language.isoEnglishen_US
dc.publisherBentham Science Publishers B.V.en_US
dc.relation.ispartofseriesCurrent Pharmaceutical Analysis
dc.relation.ispartofseries14
dc.subjectOctober University for Modern Sciences and Arts
dc.subjectجامعة أكتوبر للعلوم الحديثة والآداب
dc.subjectUniversity of Modern Sciences and Arts
dc.subjectMSA University
dc.subjectCRACLSen_US
dc.subjectDantrolene sodiumen_US
dc.subjectMCR-ALSen_US
dc.subjectParacetamolen_US
dc.subjectPLSen_US
dc.subjectStability indicating methodsen_US
dc.subjectdantroleneen_US
dc.subjectparacetamolen_US
dc.subjectArticleen_US
dc.subjectchemometricsen_US
dc.subjectconcentration residuals augmented classical least squaresen_US
dc.subjectcontrolled studyen_US
dc.subjectdrug determinationen_US
dc.subjectdrug impurityen_US
dc.subjectdrug stabilityen_US
dc.subjectleast square analysisen_US
dc.subjectmultivariate curve resolution alternating least squaresen_US
dc.subjectpartial least squares regressionen_US
dc.subjectpractice guidelineen_US
dc.subjectpriority journalen_US
dc.subjectqualitative analysisen_US
dc.subjectquantitative analysisen_US
dc.titleQualitative and quantitative chemometry as stability-indicating methods for determination of dantrolene sodium and paracetamolen_US
dc.typeArticleen_US
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